• July 16, 2018

Siren Cold Process Soap Tutorial

This cold process soap is inspired by the colors and textures of the ocean, mermaids, and sirens. It’s scented with new Pacific Pearl Fragrance Oil from the Seascape Collection. To make the top look like mermaid scales, soap is dotted on with a squeeze bottle and smoothed out with a spoon.

We first tackled this technique in 2015 with the Mermaid Tail Cold Process Soap. For that recipe, we created separate batches for the base and scales so the soap stayed thin enough to pipe. This tutorial uses one large batch, but you still have plenty of time to work. Make sure to stick blend sparingly and use a well-behaved fragrance oil.

Siren Cold Process Soap DIY

Creating the mermaid scales isn’t necessarily hard, but it takes a little practice to get the feel for it. The soap needs to be firm enough to hold its shape but fluid enough to squeeze out easily. If you don’t have squeeze bottles, you can also use frosting bags. Below are a few videos that show this technique in action.

Siren Cold Process Soap

What You Need:
5 Pound Mold with Sliding Bottom
Silicone Liner for 5 lb Wood Mold
Squeeze Bottles
1.2 oz. Castor Oil (2%)
16.2 oz. Coconut Oil (27%)
4 oz. Meadowfoam Oil (6.7%)
16.2 oz. Olive Oil (27%)
16.2 oz. Palm Oil (27%)
6.2 oz. Sweet Almond Oil (10.3%)
8.4 oz. Sodium Hydroxide Lye
18.8 oz. Distilled Water (5% water discount)
4 oz. Pacific Pearl Fragrance Oil
Hydrated Chrome Green Pigment
Titanium Dioxide
Black Oxide Pigment
Super Pearly White Mica in a Powder Sprayer

Click below to add everything you need for this project to your Bramble Berry shopping cart!

How to Make Siren Cold Process Soap

If you’ve never made cold process soap before, stop here. We highly recommend checking out our FREE four part SoapQueen.tv series on cold process soapmaking, especially the episode on lye safety. And if you’d rather do some reading, Bramble Berry carries a wide range of books on the topic, including Pure Soapmaking. You can also check out the digital downloads for that instant gratification factor.

FRAGRANCE PREP: Measure 4 ounces of Pacific Pearl Fragrance Oil into a small glass container and set aside.

COLORANT PREP: Disperse 3 teaspoons of titanium dioxide into 3 tablespoons of a lightweight liquid oil such as sunflower or sweet almond oil. Disperse 1/2 teaspoon Black Oxide Pigment into 1/2 tablespoon of lightweight liquid oil. Then, disperse 2 teaspoons of Hydrated Chrome Green Pigment with 2 tablespoon of lightweight oil. Use a mini mixer to get rid of clumps.
Optional: To ensure the titanium dioxide blends smoothly into the soap, we recommend micronizing it before dispersing it in oil. Use a coffee grinder to break up any clumps of color and prevent streaks of white from showing in the final soap. We like to use a coffee grinder that has a removable stainless steel mixing area for easy cleaning. 

SAFETY FIRST: Suit up for safe handling practices. That means goggles, gloves, and long sleeves. Make sure kids, pets, other distractions, and tripping hazards are out of the house or don’t have access to your soaping space. Always soap in a well-ventilated area.

ONE: Slowly and carefully add 8.4 ounces of lye to 18.8 ounces of distilled water. Gently stir until the lye has fully dissolved. Set it aside to cool. If you’d like a harder bar of soap that releases faster from the mold, you can add sodium lactate to the cooled lye water. Use 1 teaspoon of sodium lactate per pound of oils in the recipe. For this recipe, you’d add 4 teaspoons sodium lactate.

TWO: Melt and combine 1.2 ounces of castor oil, 16.2 ounces of coconut oil, 4 ounces of meadowfoam oil, 6.2 ounces of sweet almond oil, 16.2 ounces of olive oil, and 16.2 ounces of palm oil (remember to fully melt then mix your entire container of palm oil before portioning) into a large mixing bowl. Once the lye water and the oils have cooled to 130 degrees F or below (and are ideally within 10 degrees of each other), add the lye water to the oils and stick blend the mixture to a thin trace.

ONETWO

THREE: Split the soap batter into four separate containers. Two containers should contain 600 mL, and the other two containers should contain 700 mL.

FOUR: Add the following amounts of dispersed colorants to each container and use a whisk to incorporate.

  • Container A – lightest green (700 mL): 2 tablespoons dispersed titanium dioxide + 1/2 teaspoon dispersed Hydrated Chrome Green Pigment
  • Container B – light green (600 mL): 1 teaspoon dispersed titanium dioxide + 1/2 teaspoon Hydrated Chrome Green Pigment
  • Container C – medium green (700 mL): 1 teaspoon dispersed Hydrated Chrome Green Pigment
  • Container D – darkest green (600 mL): 1.5 teaspoons dispersed Hydrated Chrome Green Pigment + about 1/8 teaspoon dispersed Black Oxide Pigment

THREEFOUR

FIVE: Add the 4 ounces of Pacific Pearl Fragrance Oil evenly to each container (it’s okay to eyeball it).

FIVE

SIX: Pour about 100-150 mL of the lightest green soap (container A) and 100-150 mL of the medium green soap (container C) into the squeeze bottles. Screw on the lids and set aside.

ELEVEN1

SEVEN: If the soap is still at a thin trace, stick blend each container from lightest to darkest until all four colors are a medium trace. Pour all of the darkest green soap into the mold. Use a spoon to create peaks and divots into the soap.

SIXSEVEN

EIGHT: Pour all of the medium green soap into the mold. Tap firmly on the counter to get rid of bubbles, then use a spoon to create peaks and divots into the medium green soap layer.

EIGHT

NINE: Pour all of the light green soap into the mold. Tap firmly on the counter to get rid of bubbles, then use a spoon to create peaks and divots into the light green soap layer.

NINE

TEN: Pour all of the lightest green soap into the mold. It will fill to the very top of the silicone liner. Use a large spoon or spatula to evenly spread the soap to create a smooth and even base to create the scales.

TENTEN2

Create the Scales/Petals

This technique involves squeezing dots of soap and then using a spoon to lightly press and slide down. The soap should be thin enough that it can be squeezed out of the bottles, but thick enough that it holds its shape.

To get the feel for it, you may want to practice a few scales on a paper towel. If the soap doesn’t come out easily, cut a small portion of the squeeze bottle tip off to create a larger hole.

You’ll also need a spoon with a slightly pointed tip. If the spoon tip is too round, it may be difficult to create the scales. Make sure your spoon is not aluminum, which reacts with the lye and creates toxic fumes. You will also need paper towels on hand to clean off the spoon in between different colors of scales.

ELEVEN

ELEVEN: Working quickly, create five dots of color across the top of the mold, swapping the color with each dot. The dots should just touch. Once you have placed five dots, Use the spoon to gently press each dot of color, sliding the spoon toward you. Between each color, clean off the spoon on the paper towel or rag.
NOTE: In the photos below, you can see that in the first row we placed six dots. We found this to be a little bit tight, and switched to only five dots in the next layer. 

TWELVETHIRTEEN

TWELVE: In the second row, switch the color order so that you squeeze a light green dot onto a dark green dot in the layer above, and vice versa. Use the spoon to gently press each dot of color, sliding the spoon toward you. Continue swapping the color order for each row.
TIP: To keep the process going as quickly as possible, squeeze one color of dots first, and fill in the row with the other color. This eliminates picking up the bottles as often, and helps speed the process along. 

FOURTEENFIFTEENSIXTEEN

THIRTEEN: As you work, the soap will continue to thicken. This is why it’s important to work carefully but also quickly. Don’t worry about each scale being completely perfect.

Once we got to about the middle of the mold, our soap was getting quite thick. It was still workable, but required us to tap the squeeze bottle on the counter to transfer the soap to the top of the bottle. We also cut off the very tip to produce a larger hole for the soap to be squeezed through. SEVENTEENEIGHTEENNINETEEN

FOURTEEN: Continue squeezing scales until you reach the very end of the mold.

TWENTY

FIFTEEN: Once the top is completely decorated, use the powder sprayed filled with Super Pearly White Mica to dust a light layer on top. It’s tricky to see in photos, but the mica really makes the scales pop.

TWENTYONE

SIXTEEN: Spray the soap with 99% isopropyl alcohol to prevent soda ash. To promote gel phase, place the soap on a heating pad set to medium for 30-60 minutes. To help insulate, we bent a piece of cardboard and placed it over the mold without touching the top. Allow it to stay covered for at least 6 hours. Keep an eye on it to make sure it doesn’t get too hot and crack. If you see a crack starting to form, take it off the heating pad and remove any insulation.

TWENTYTWO

After about 1-3 days (depending if sodium lactate was used or not), remove the soap from the mold and silicone liner. Cut into thick bars to allow 2 rows of scales to be seen in each bar. After cutting, allow them to cure for 4-6 weeks and enjoy.

We used the Soap Beveller to finish these bars. Below, you can see the difference between beveled and non-beveled soap.

Bevel vs Unbevel

 

Siren Cold Process Soap Tutorial

Soap Queen
Cook Time 3 hours
Total Time 3 hours
Recipe type Cold process soap
Makes 5 1/2 pounds of soap

Ingredients
  

  • 5 Pound Mold with Sliding Bottom
  • Silicone Liner for 5 lb Wood Mold
  • 2 Squeeze Bottles
  • 1.2 oz. Castor Oil 2%
  • 16.2 oz. Coconut Oil 27%
  • 4 oz. Meadowfoam Oil 6.7%
  • 16.2 oz. Olive Oil 27%
  • 16.2 oz. Palm Oil 27%
  • 6.2 oz. Sweet Almond Oil 10.3%
  • 8.4 oz. Sodium Hydroxide Lye
  • 18.8 oz. Distilled Water 5% water discount
  • 4 oz. Pacific Pearl Fragrance Oil
  • Hydrated Chrome Green Pigment
  • Titanium Dioxide
  • Black Oxide Pigment
  • Super Pearly White Mica in a Powder Sprayer

Instructions
 

FRAGRANCE PREP: Measure 4 ounces of Pacific Pearl Fragrance Oil into a small glass container and set aside.

    COLORANT PREP: Disperse 3 teaspoons of titanium dioxide into 3 tablespoons of a lightweight liquid oil such as sunflower or sweet almond oil. Disperse 1/2 teaspoon Black Oxide Pigment into 1/2 tablespoon of lightweight liquid oil. Then, disperse 2 teaspoons of Hydrated Chrome Green Pigment with 2 tablespoon of lightweight oil. Use a mini mixer to get rid of clumps.

    • Optional: To ensure the titanium dioxide blends smoothly into the soap, we recommend micronizing it before dispersing it in oil. Use a coffee grinder to break up any clumps of color and prevent streaks of white from showing in the final soap. We like to use a coffee grinder that has a removable stainless steel mixing area for easy cleaning.

    SAFETY FIRST: Suit up for safe handling practices. That means goggles, gloves, and long sleeves. Make sure kids, pets, other distractions, and tripping hazards are out of the house or don’t have access to your soaping space. Always soap in a well-ventilated area.

    • Slowly and carefully add 8.4 ounces of lye to 18.8 ounces of distilled water. Gently stir until the lye has fully dissolved. Set it aside to cool. If you’d like a harder bar of soap that releases faster from the mold, you can add sodium lactate to the cooled lye water. Use 1 teaspoon of sodium lactate per pound of oils in the recipe. For this recipe, you’d add 4 teaspoons sodium lactate.
    • Melt and combine 1.2 ounces of castor oil, 16.2 ounces of coconut oil, 4 ounces of meadowfoam oil, 6.2 ounces of sweet almond oil, 16.2 ounces of olive oil, and 16.2 ounces of palm oil (remember to fully melt then mix your entire container of palm oil before portioning) into a large mixing bowl. Once the lye water and the oils have cooled to 130 degrees F or below (and are ideally within 10 degrees of each other), add the lye water to the oils and stick blend the mixture to a thin trace.
    • Split the soap batter into four separate containers. Two containers should contain 600 mL, and the other two containers should contain 700 mL.
    • Add the following amounts of dispersed colorants to each container and use a whisk to incorporate.
      Container A – lightest green (700 mL): 2 tablespoons dispersed titanium dioxide + 1/2 teaspoon dispersed Hydrated Chrome Green Pigment
      Container B – light green (600 mL): 1 teaspoon dispersed titanium dioxide + 1/2 teaspoon Hydrated Chrome Green Pigment
      Container C – medium green (700 mL): 1 teaspoon dispersed Hydrated Chrome Green Pigment
      Container D – darkest green (600 mL): 1.5 teaspoons dispersed Hydrated Chrome Green Pigment + about 1/8 teaspoon dispersed Black Oxide Pigment
    • Add the 4 ounces of Pacific Pearl Fragrance Oil evenly to each container (it’s okay to eyeball it).
    • Pour about 100-150 mL of the lightest green soap (container A) and 100-150 mL of the medium green soap (container C) into the squeeze bottles. Screw on the lids and set aside.
    • If the soap is still at a thin trace, stick blend each container from lightest to darkest until all four colors are a medium trace. Pour all of the darkest green soap into the mold. Use a spoon to create peaks and divots into the soap.
    • Pour all of the medium green soap into the mold. Tap firmly on the counter to get rid of bubbles, then use a spoon to create peaks and divots into the medium green soap layer.
    • Pour all of the light green soap into the mold. Tap firmly on the counter to get rid of bubbles, then use a spoon to create peaks and divots into the light green soap layer.
    • Pour all of the lightest green soap into the mold. It will fill to the very top of the silicone liner. Use a large spoon or spatula to evenly spread the soap to create a smooth and even base to create the scales.

    Create the Scales/Petals

    • Working quickly, create five dots of color across the top of the mold, swapping the color with each dot. The dots should just touch. Once you have placed five dots, Use the spoon to gently press each dot of color, sliding the spoon toward you. Between each color, clean off the spoon on the paper towel or rag. NOTE: In the photos below, you can see that in the first row we placed six dots. We found this to be a little bit tight, and switched to only five dots in the next layer.
    • In the second row, switch the color order so that you squeeze a light green dot onto a dark green dot in the layer above, and vice versa. Use the spoon to gently press each dot of color, sliding the spoon toward you. Continue swapping the color order for each row. TIP: To keep the process going as quickly as possible, squeeze one color of dots first, and fill in the row with the other color. This eliminates picking up the bottles as often, and helps speed the process along.
    • As you work, the soap will continue to thicken. This is why it’s important to work carefully but also quickly. Don’t worry about each scale being completely perfect. Once we got to about the middle of the mold, our soap was getting quite thick. It was still workable, but required us to tap the squeeze bottle on the counter to transfer the soap to the top of the bottle. We also cut off the very tip to produce a larger hole for the soap to be squeezed through.
    • Continue squeezing scales until you reach the very end of the mold.
    • Once the top is completely decorated, use the powder sprayed filled with Super Pearly White Mica to dust a light layer on top. It’s tricky to see in photos, but the mica really makes the scales pop.
    • Spray the soap with 99% isopropyl alcohol to prevent soda ash. To promote gel phase, place the soap on a heating pad set to medium for 30-60 minutes. To help insulate, we bent a piece of cardboard and placed it over the mold without touching the top. Allow it to stay covered for at least 6 hours. Keep an eye on it to make sure it doesn’t get too hot and crack. If you see a crack starting to form, take it off the heating pad and remove any insulation.
    • After about 1-3 days (depending if sodium lactate was used or not), remove the soap from the mold and silicone liner. Cut into thick bars to allow 2 rows of scales to be seen in each bar. After cutting, allow them to cure for 4-6 weeks and enjoy. We used the Soap Beveller to finish these bars. Below, you can see the difference between beveled and non-beveled soap.
    Tried this recipe?Let us know how it was!

     

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    1. I haven’t made soap for about 15 years and then it was just melt and pour so if I sound ignorant please excuse me. I read all through the instructions and was left with 4 questions: 1. How hot should the distilled water be to dissolve the Lye? 2. is the coconut oil solid or fractionated? 3. What is meant by the term “trace” it says thin or medium trace. and lastly . Can essential oils be used in place of the fragrance oil?Thank you for the clarification. I’m excited to learn something new.

      1. The distilled water should be room temperature it is the lye reaction that heats it up. Since you are just getting started with cold process soap I would recommend watching this series on the basics before getting started:
        https://www.youtube.com/playlist?list=PLAADF6209996265D2

        We used regular 76 degree Coconut Oil, if using another kind the recipe will mention that.
        Coconut Oil: https://www.brambleberry.com/Coconut-Oil-P3196.aspx

        Trace is when your soap is starting to come together into a soap batter. Find out more about trace here:
        https://soapqueen.com/bath-and-body-tutorials/tips-and-tricks/trace/

        You can use essential oils instead of fragrance oils just keep in mind they may perform differently. We normally list performance notes on their product pages. Find out how much to use with our Fragrance Calculator:
        https://www.brambleberry.com/Pages/Fragrance-Calculator.aspx

    2. Is there anything I can substitute for palm oil? I do not use it b/c of the environmental issues it’s creating. Thanks!

    3. 4 stars
      I love this soap! It’s gorgeous! I decided to try it out except I used different colors and I didn’t do the top like that (no patience tonight). In fact I’m still in the process of making it because my batter wouldn’t thicken up as I anticipated. I used this recipe except I used avocado instead of meadowfoam because I didn’t have any. The first layer is colored with yellow silt clay and it took about 45 minutes to thicken just enough so I could texture it. The next two layers weren’t bad using mica and I just put the fourth layer on (white) and am waiting for that to thicken so I can texture the top. I used full water because I was afraid it would accelerate way to fast for me to work with but it was just the opposite. I’ve never really used clay before as a colorant so could that have been the cause of not thickening? I don’t understand the white with the td because td always seems to make my batter thicker. Any idea what went wrong? Feels like I’ve been doing this for five hours lol
      Thanks!

      1. That is really odd that you didn’t have it thicken up on you like expected. It definitely should have, especially since clays typically thicken up soap batter. How old is your lye? If it is older than a year sometimes you will have to work longer and harder to get your batter to thicken up. It could also be a Potassium vs Sodium Hydroxide mix. Did you use Potassium Hydroxide instead of Sodium?

    4. How can I adjust this soap to make in my 10” silicone BB soap mold? (I’m still learning )

      1. I’m sure BB will offer some great advice, but I’ve done this several times. When Soapqueen uses this 5 lb mold and I want to use it for my 10″ BB mold, I reduce each and every oil by 33% THEN ALWAYS run the new recipe through the lye calculator. You will have to reduce the amount of colors, too, but the BB website gives recommendations on amounts to use. I plan to do this very thing with this soap in the next few weeks so I hope this helps you!

    5. 5 stars
      Very nice soap!! How many soaps the does the mold give you? Also if I want to sell a soap, do you have an idea of a price? I think my calculation is off, thanks!

    6. The soap looks great! You folks must have the patience of Jobe to do that top on that large mold!

      1. Thanks, Eric. It definitely took a lot of patience, but it was worth it.

    7. 5 stars
      This is a beautiful soap. These colors have always been one of my favorite color schemes, and I absolutely love the ombre effect.

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